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Beilstein J. Org. Chem. 2013, 9, 974–982, doi:10.3762/bjoc.9.112
Graphical Abstract
Scheme 1: Appel-reagent-mediated transformation of glycosyl hemiacetal derivatives into thioglycosides and β-...
Scheme 2: Plausible mechanistic pathways for the formation of 1,2-trans-thioglycoside and β-glycosyl thiol.
Beilstein J. Org. Chem. 2013, 9, 74–78, doi:10.3762/bjoc.9.9
Scheme 1: Removal of benzylidene acetal and benzyl ether by using a combination of triethylsilane and 10% Pd/...
Beilstein J. Org. Chem. 2011, 7, 1182–1188, doi:10.3762/bjoc.7.137
Figure 1: Structure of the tetrasaccharide repeating unit of the O-antigen of Shigella boydii type 9.
Figure 2: Structure of the synthesized tetrasaccharide and its intermediates.
Scheme 1: Reagents: (a) acetic anhydride, sulfamic acid, 60 °C, 30 min, 91%; (b) Et3SiH, I2, 0–5 °C, 30 min, ...
Scheme 2: Reagents: (a) HClO4–SiO2, CH2Cl2, −15 °C, 1 h, 81%; (b) benzyl bromide, NaOH, n-Bu4NBr, THF, rt, 2 ...
Scheme 3: Reagents: (a) N-iodosuccinimide, HClO4–SiO2, −10 °C, 1 h, 82%; (b) 0.1 M CH3ONa, CH3OH, rt, 3 h; (c...